XPS资料：XPS文献分析.pptx

XPSXPS文献分析文献分析SHUSHU等离子体修饰聚合物表面的XPS分析1聚合物老化的XPS分析2表面涂层的XPS分析3大纲纲1 1SHUSHUThe effect of oxygen-plasma treatment on Kevlar fibers and the properties ofKevlar fibers/bismaleimide compositesMin SuAijuan GuGuozheng Liang Li Yuan等离子体修饰聚合物表面的XPS分析2 2SHUSHU等离子体修饰聚合物表面的XPS分析1.1研究背景图1 凯夫拉纤维的结构式图2 a 凯夫拉纤维的SEM照片；b 经过氧等离子体处理的凯夫拉纤维SEM照片Su M, Gu A, Liang G, et al. The effect of oxygen-plasma treatment on Kevlar fibers and the properties of Kevlar fibers/bismaleimide compositesJ. Applied Surface Science, 2011, 257(8): 3158-3167.3 3SHUSHU等离子体修饰聚合物表面的XPS分析Su M, Gu A, Liang G, et al. The effect of oxygen-plasma treatment on Kevlar fibers and the properties of Kevlar fibers/bismaleimide compositesJ. Applied Surface Science, 2011, 257(8): 3158-3167.1.2结果讨论图3 经过不同时间等离子体处理和未经处理的KF的XPS谱图4 4SHUSHU等离子体修饰聚合物表面的XPS分析Su M, Gu A, Liang G, et al. The effect of oxygen-plasma treatment on Kevlar fibers and the properties of Kevlar fibers/bismaleimide compositesJ. Applied Surface Science, 2011, 257(8): 3158-3167.1.2结果讨论图4 未经处理的凯夫拉纤维的XPS谱图5 5SHUSHU等离子体修饰聚合物表面的XPS分析Su M, Gu A, Liang G, et al. The effect of oxygen-plasma treatment on Kevlar fibers and the properties of Kevlar fibers/bismaleimide compositesJ. Applied Surface Science, 2011, 257(8): 3158-3167.1.2结果讨论图5 经过处理的凯夫拉纤维的XPS谱图6 6SHUSHU等离子体修饰聚合物表面的XPS分析Su M, Gu A, Liang G, et al. The effect of oxygen-plasma treatment on Kevlar fibers and the properties of Kevlar fibers/bismaleimide compositesJ. Applied Surface Science, 2011, 257(8): 3158-3167.1.2结果讨论图6 经过不同处理时间的凯夫拉纤维的XPS谱图7 7SHUSHU等离子体修饰聚合物表面的XPS分析Su M, Gu A, Liang G, et al. The effect of oxygen-plasma treatment on Kevlar fibers and the properties of Kevlar fibers/bismaleimide compositesJ. Applied Surface Science, 2011, 257(8): 3158-3167.1.2结果讨论表 1 未经处理和经过处理的凯夫拉纤维表面的的化学组成和官能团8 8SHUSHU等离子体修饰聚合物表面的XPS分析Su M, Gu A, Liang G, et al. The effect of oxygen-plasma treatment on Kevlar fibers and the properties of Kevlar fibers/bismaleimide compositesJ. Applied Surface Science, 2011, 257(8): 3158-3167.1.2结果讨论图7 经过处理的凯夫拉纤维老化0天的XPS谱图9 9SHUSHUSu M, Gu A, Liang G, et al. The effect of oxygen-plasma treatment on Kevlar fibers and the properties of Kevlar fibers/bismaleimide compositesJ. Applied Surface Science, 2011, 257(8): 3158-3167.1.2结果讨论图8 经过处理的凯夫拉纤维老化15天的XPS谱图等离子体修饰聚合物表面的XPS分析1010SHUSHUSu M, Gu A, Liang G, et al. The effect of oxygen-plasma treatment on Kevlar fibers and the properties of Kevlar fibers/bismaleimide compositesJ. Applied Surface Science, 2011, 257(8): 3158-3167.1.2结果讨论图9 经过处理的凯夫拉纤维老化的XPS谱图a老化0天；b老化5天；c老化10天；d老化15天等离子体修饰聚合物表面的XPS分析1111SHUSHUSu M, Gu A, Liang G, et al. The effect of oxygen-plasma treatment on Kevlar fibers and the properties of Kevlar fibers/bismaleimide compositesJ. Applied Surface Science, 2011, 257(8): 3158-3167.表 2 经过处理凯夫拉纤维表面老化的的化学组成和官能团1.2结果讨论等离子体修饰聚合物表面的XPS分析1212SHUSHUSu M, Gu A, Liang G, et al. The effect of oxygen-plasma treatment on Kevlar fibers and the properties of Kevlar fibers/bismaleimide compositesJ. Applied Surface Science, 2011, 257(8): 3158-3167.小结通过过氧等离子体修饰凯饰凯 夫拉纤维纤维 的XPS谱图谱图 分析，我们发现们发现 氧等离子体表面改性的效果良好，通过过剪切强度等试验发现试验发现 与理论论的预预期效果相符合。

通过过XPS分析氧等离子体处处理凯凯夫拉纤维纤维 表面老化的情况，说说明老化现现象并不严严重等离子体修饰聚合物表面的XPS分析1313SHUSHU聚合物老化的XPS分析Study of polypyrrole aging by XPS, FTIR and conductivity measurementsJan a Tabaiarov,Matej Miuk ,Pavol Fedorko,Mria Omastov1414SHUSHU2.1研究背景图10 聚吡咯分子结构示意图图11 掺杂聚吡咯分子导电结构示意图聚合物老化的XPS分析Tabaiarov J, Miuk M, Fedorko P, et al. Study of polypyrrole aging by XPS, FTIR and conductivity measurementsJ. Polymer Degradation and Stability, 2015, 120: 392-401.1515SHUSHU聚合物老化的XPS分析Tabaiarov J, Miuk M, Fedorko P, et al. Study of polypyrrole aging by XPS, FTIR and conductivity measurementsJ. Polymer Degradation and Stability, 2015, 120: 392-401.2.2结果讨论图12 PPy-Cl样品的XPS能谱图像的a)C1s峰位和b)C1s的峰型1616SHUSHU聚合物老化的XPS分析Tabaiarov J, Miuk M, Fedorko P, et al. Study of polypyrrole aging by XPS, FTIR and conductivity measurementsJ. Polymer Degradation and Stability, 2015, 120: 392-401.2.2结果讨论图13 PPy-Cl的XPS谱图1717SHUSHU聚合物老化的XPS分析Tabaiarov J, Miuk M, Fedorko P, et al. Study of polypyrrole aging by XPS, FTIR and conductivity measurementsJ. Polymer Degradation and Stability, 2015, 120: 392-401.2.2结果讨论图13 PPy-Cl2的XPS谱图1818SHUSHU聚合物老化的XPS分析Tabaiarov J, Miuk M, Fedorko P, et al. Study of polypyrrole aging by XPS, FTIR and conductivity measurementsJ. Polymer Degradation and Stability, 2015, 120: 392-401.2.2结果讨论图13 PPy-Cl-DBS的XPS谱图1919SHUSHU聚合物老化的XPS分析Tabaiarov J, Miuk M, Fedorko P, et al. Study of polypyrrole aging by XPS, FTIR and conductivity measurementsJ. Polymer Degradation and Stability, 2015, 120: 392-401.2.2结果讨论图13 PPy-SO4的XPS谱图2020SHUSHU聚合物老化的XPS分析Tabaiarov J, Miuk M, Fedorko P, et al. Study of polypyrrole aging by XPS, FTIR and conductivity measurementsJ. Polymer Degradation and Stability, 2015, 120: 392-401.2.2结果讨论图13 PPy-S2O8的XPS谱图2121SHUSHU聚合物老化的XPS分析Tabaiarov J, Miuk M, Fedorko P, et al. Study of polypyrrole aging by XPS, FTIR and conductivity measurementsJ. Polymer Degradation and Stability, 2015, 120: 392-401.2。